By S. Velumani and René Asomoza
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Additional info for Advances in Semiconducting Materials
1, that the height of the preferential peak increases and some new peaks of CdSe begin to appear while increasing bath temperature from 30 to 800C. It is also observed that the crystallites are preferentially oriented along (002) plane. An aggregate of distorted crystallites as a measure of the particle size and strain could affect the variance of the x-ray diffraction line profiles. Since the method is sensitive to the variation near the tails of the peaks, a careful adjustment of the background was carried out following the method of Mitra and Misra .
Previous investigations reported that cracks in many ceramics were healed by heat-treatment. ; increase in reliability of ceramic elements, decrease of maintenance costs and prolonged lifetime of components. Lange  and Gupta  reported that crack healing process in monolithic alumina was induced not by intrinsic crack healing but by a mechanism similar to the densification during sintering. By contrast, structural ceramics containing SiC as sintering additive or reinforcement have been crack healed by reaction of SiC and the O2 in the atmosphere, as reported in the case of Al2O3/SiC [1, 12, S.
9%, mean grain size of 200 nm) as the source material for Ni particles were selected. Ni/Al2O3 nanocomposite was prepared by an aqueous solution method, the content of Ni in the final composite was fixed to be 5 vol%. The slurry of α-Al2O3 powder and Ni nitrate in water was dried at 300ºC and then reduced by raising temperature to 600ºC with a heating rate of 400 K / h for 12 h in a stream of Ar + 1%H2 gas mixture. The nanocomposite powder was sintered to a disc (15 mm diameter x 4 mm thickness) using pulsed electric current sintering (PECS) at 1400ºC for 5 min in vacuum under uniaxial pressure of 45 MPa.